9-fluorenone was isolated and purified from a crude mixture containing chloroanilic acid and benzocaine dissolved in diethyl ether. Arrange the various steps carried out experiment:

a. Drain off the remaining organic from the tip of the separatory funnel
b. Weight out the product and determine Its MP
c. Mix/vent then drain off the organic layer
d. Add sodium sulfate to the aqueous layer to remove aw residua' water
e. Add the crude reaction mixture to the separatory funnel
f. Extract chloroaniIic acid by adding 5%. HCl solution to the crude reaction mixture
g. Extract benzociane by adding 5% HCI solution to the crude reaction mixture
h. Decant the into a round bottom flask and use the rotavap to evaporate solvent
i. Extract benzociane by adding 5% NaOH solution to the organic layer
j. Extract chloroanilic acid by 5% NaOH to to organic War
k. Add sodium sulfate to the organic layer to remove any residual water
l. Mix/vent then drain off the aqueous layer

Answers

Answer 1

Answer:

Explanation:

[tex]\text{The steps shown below indicate the rearrangement of the experiment.}[/tex]

[tex]\text{e. Add the crude reaction mixture to the separatory funnel}[/tex]

[tex]\text{f. Extract chloroaniIic acid by adding 5\%. HCl solution to the crude reaction mixture }[/tex]

[tex]\text{l. Mix/vent then drain off the aqueous layer}[/tex]

[tex]\text{i. Extract benzociane by adding 5\% NaOH solution to the organic layer}[/tex]

[tex]\text{c. Mix/vent then drain off the organic layer}[/tex]

[tex]\text{d. Add sodium sulfate to the aqueous layer to remove aw residual water}[/tex]

[tex]\text{a. Drain off the remaining organic from the tip of the separatory funnel}[/tex]

[tex]\text{h. Decant the into a round bottom flask and use the rotavap to evaporate solvent}[/tex]

[tex]\text{b. Weight out the product and determine Its MP}[/tex]


Related Questions

Write True if the statement is correct and False if it is incorrect.
1. Mosquitos are flies.
2. All large invertebrates live in the
sea or at least in water.
3. An arthropod is a form of arachnid.
4. The giant squid is the world's largest
invertebrate.
5. Earthworms have skeleton
6. The octopus is the most advance of
the mollusks.
7. Insects are vertebrates animals.
8. Starfish have shells.
9. Snails have spiral protective shell.
10. Ants and termites both live in colonies
with a complex social structure.​

Answers

T
F
F
T
F
T
T
F
T
T...............................

A per the statement the true and false have been stated.

The mosquitos are flies is True. All large invertebrates live in the sea or at least in water is False. An arthropod is a form of arachnid. False. The giant squid is the world's largest  invertebrate is true. Earthworms have skeleton is false. An octopus is the most advance of  the mollusks is True. Insects are vertebrates animals is false . Most starfish have shells is true.   All Snails have a spiral protective shell is true. The Ants and the termites both live in their colonies  with a complex social structure true.

Learn more about the statement is correct and False if it is incorrect.

brainly.com/question/25942470.

Can someone help me with these two?

Answers

Answer:

adding

opposite

Explanation:

dont blame me if u get them wrong

Answer:

first one is adding i belive and second one is opposite

Explanation:

describe how the root systems of the mesquite tree and saguaro cactus root systems different. PLZ help me

Answers

Answer:

the mesquite trees roots go down into the grown, while the saguaro cactus is going to the sides.

Arrange the liquids pentane (CH3CH2CH2CH2CH3), pentanol (CH3CH2CH2CH2CH2OH), and pentanal (CH3CH2CH2CH2CHO) in order of decreasing viscosity, surface tension, and boiling point.

Rank from highest to lowest viscosity, surface tension, and boiling point.

Answers

Answer:

Following are decreasing order to this question:

Explanation:

Viscosity and surface tension both are inter-molecular by nature (IMFs)

The pentane becomes non-polar and just not H-bondable, so LDF alone would be likely (London Dispersion Force)

Pentanal, but H-bond => is impossible (Dipole-Dipole)

Pentanol is also an OH group, so H-bond => is probable (Hydrogen Bonding)

Higher air tension and viscosity than higher IMFs (because the atoms of fluids are more drawn). To lower the IMF (and therefore the viscosity/surface stress decreases)

pentanol

pentanal

pentane

A tank contains one hundred fifty kmol of an aqueous phosphoric acid solution with 5.00 mole% H3PO4. The solution is concentrated by adding pure phosphoric acid at a rate of 30.0 L/min. Molecular weight of phosphoric acid is 98. Density of phosphoric acid is 1.834 kg/L. Determine the mole fraction of phosphoric acid in the tank at 25 minutes.

Answers

Answer:

Mole fraction  = 0.1313

Explanation:

given data

Addition rate of pure phosphoric acid = 30L/min

Phosphoric acid added in 25 min = 750 L

solution

mass is express as here

mass = density × volume and number of moles = mass ÷ molar mass

So, In terms of moles

phosphoric acid added = (750 × 1.834) ÷ 98

phosphoric acid added = 14.036 kmol

and

moles of phosphoric acid in tank = 0.05 × 150 + 14.036

moles of phosphoric acid in tank = 21.536 kmol

and

Moles of water in tank = 0.95 × 150

Moles of water in tank = 142.5 kmol

So that Mole fraction of phosphoric acid in tank

Mole fraction = 21.536 ÷ (21.536+142.5)

Mole fraction  = 0.1313

MQ : Which parts of the brain had most likely been affected?

Answers

Answer:

the cerebrum

Explanation:

answer is A

What type is hydropower?

Answers

Answer:

Hydroelectric energy, also called hydroelectricity or hydropower, is a form of energy that uses the power of flowing water to generate electricity. There are three main types of hydroelectric energy: impoundment, diversion, and pumped storage.

Explanation:

A 50.8g sample of glass, which has a specific heat capacity of 0.670·J·g?1°C?1, is put into a calorimeter (see sketch at right) that contains 150.0g of water. The temperature of the water starts off at 22.0°C. When the temperature of the water stops changing it's 25.6°C. The pressure remains constant at 1atm. Calculate the initial temperature of the glass sample. Be sure your answer is rounded to the correct number of significant digits.

Answers

Answer:

Explanation:

mass of glass m = 50.8 g

specific heat s = .67 J /g °C

initial temperature = t

Loss of heat by glass

= m s Δ t

= 50.8 x .67 x ( t - 25.6 )

= 34.036 x ( t - 25.6 )

Gain of heat by water

= 150 x 4.2 x ( 25.6 - 22.0 )

= 2268

Heat gain = heat lost

2268 = 34.036 x ( t - 25.6 )

2268 = 34.036  t - 871.32

34.036 t = 3139.32

t = 92.23°C .  


Is this answer correct

Answers

Answer:

Yes

Explanation:

Would you expect a reaction to occur with Hydrogen gas and Copper (II) chloride?

Answers

Yes

The copper itself can react with hydrogen

Here is the chemical reaction

2CuCl2(aq) + H2(g) -> 2CuCl(s) + 2HCl(g)

Which of the following molecules is least soluble in water?​

Answers

Answer:

CCl4

Explanation:

Because it is non polar and non polar substances are insoluble in water.

The molecule which is least soluble in water is C(Cl)₄

Which molecules are soluble in water?

Water is polar molecule and only polar molecules are soluble in water.

(CH₃)₂CO is a polar molecule as due to partial positive and negative charges on carbon and oxygen atom as a result of which it is soluble in water.C(Cl)₄ is a non polar molecule as net dipole moment of the molecule is zero, so it is insoluble in water.CH₃OH is also polar molecule and shows solubility in water.(CH₃)₂O is also polar and dissolve in water.

Hence tetra chloro carbon is insoluble in water.

To know more about solubility, visit the below link:

https://brainly.com/question/16903071

#SPJ2

Why does there appear to be another duck head in the water?
A
The water in the pond reflects light from the Sun, making a mirror image
B
The molecules in the atmosphere refract the light, splitting it into two ima
С
The duck scatters the light, making hundreds of tiny refractions that collec
D
The bottom of the pond absorbs the light, then projects it toward the surfa

Answers

Answer:

it's A. The water in the pond reflects light from the Sun, making a mirror image

Explanation:

i just took the test

Estimate how much heat in joules is released when 25.0 g of water (C = 4.184 J/g°C) is cooled from 80.0°C to 30.0°C?

Answers

Answer:

5230 J

Explanation:

m = 25 g = 0,025 kg

c = 4,184 J /(g * °C) = 4184 J /(kg * °C)

[tex]t_{1}[/tex] = 80 °C

[tex]t_{2}[/tex] = 30 °C

The formula is Q = c *m * ([tex]t_{2} - t_{1}[/tex])

Calculating:

Q = 4184 * 0,025 * (30 - 80) = 5230 J

Note that we get a negative heat (-5230 J). It just means that it is released.

The amount of heat will be 5230 j.

What is heat?

Heat is a type of energy that is transferred between both the system and its surroundings as a result of temperature variations.

Calculation of heat.

Given data:

Mass = 25.0 g = 0.025 kg

C = 4.184 J/g°C

[tex]T_{1}[/tex] =  80.0°C

[tex]T_{2}[/tex] = 30.0°C

Q= ?

By using the formula of heat.

Q = MC ([tex]T_{2} - T_{1}[/tex])

Put the value of given data in heat equation.

Q(heat)  = 0.025  × 4.184  ( 30 - 80)

Q(heat) = 5230 J.

Therefore, the amount of heat will be 5230 J.

To know more about heat.

https://brainly.com/question/13860901.

#SPJ2

Can someone help me please

Answers

Answer:

the answers are a, f, g

and lastly e because they all describe a liquid

MEDICAL FORENSICS

please help me i only get one chance to do this please

Answers

Answer:

i think the answer is b temperature

Answer:

no

Explanation:

Danielle is designing a system to help race cars slow safely and rapidly at her local racetrack. The racetrack is a straight, 1,000-meter stretch of asphalt. Half of the track is devoted to races and the other half is designed to let cars decelerate after crossing the finish line.

Danielle has designed a pair of small parachutes that are automatically released out the back of a car once it crosses the finish line. When her system works properly, the race car driver does not need to apply the brakes to bring the car to a stop before running out of track.

When Danielle tests a prototype of her design, it brings a race car to a stop 275 meters behind the finish line. After taking some measurements, she decides that her design causes the driver to experience too much force. To correct this, she could
A.
make the parachutes larger in order to increase the drag forces on the car and bring it to a stop 200 meters after crossing the finish line.
B.
add a third parachute in order to increase the drag forces on the car and bring it to a stop 175 meters after crossing the finish line.
C.
make the parachutes smaller in order to decrease the drag forces on the car and bring it to a stop 400 meters after crossing the finish line.
D.
remove one of the parachutes in order to decrease the drag forces on the car and bring it to a stop 550 meters after crossing the finish line.

Answers

Answer:

The answer is C

Explanation:

She should make the parachutes smaller in order to decrease the drag forces on the car and bring it to a stop 400 meters after crossing the finish line.

What happens if excess carbon dioxide is not removed from the atmosphere?

A) a decrease in the amount of fossil fuels availabe

B) it may lead to global warming

C) more dead plants and animals not decomposing before getting buried

D) increase in the amount of fossils fuels available

please help fast I need to bring my grade up I'll give 30 points.

Answers

Answer:

Carbon dioxide becomes a poisonous gas when there is too much of it in the air you breathe. Besides the effects it can have on the planet and the atmosphere, carbon dioxide poisoning can lead to central nervous system damage and respiratory deterioration in humans and other breathing creatures.

Answer:

Carbon dioxide becomes a poisonous gas when there is too much of it in the air you breathe. Besides the effects it can have on the planet and the atmosphere, carbon dioxide poisoning can lead to central nervous system damage and respiratory deterioration in humans and other breathing creatures.

Explanation:

Hope This Helps! [ :

PLEASE HELP ME ITS DUE IN 25 MINUTES True or false iron and nickel are less dense than silicates ?

Answers

The answer is false
Iron and nickel is more dense
false, iron and nickel is apart of the core in the earth. meaning it’s more dense that silicates.

What is the primary function of the chromosome?

Answers

Answer:

Store the genetic instructions needed to specify traits.

In DNA, the primary function of chromosome is store the genetic instructions needed to specify traits.

What is DNA?

DNA is a hereditary material  which is present in human beings as well as all other living organisms.  Every cell which is present in an organism's body has DNA  which is the same. Most of the DNA is situated in the cell's nucleus and small amount of it can be found in the cell's mitochondria as well.

Information which is stored in DNA is stored as codes made up of four chemical bases namely, adenine, thymine , cytosine and guanine.Human DNA consists of 3 billion bases .The order of the bases determines information which is required for building and maintaining an organism.

DNA bases are capable of pairing up with each other. Adenine pairs with thymine and guanine pairs up with cytosine .Each base is also attached to a sugar molecule  and a phosphate group. A base, phosphate  sugar are together called as nucleotides.

Learn more about DNA,here:

https://brainly.com/question/22499464

#SPJ6

The sum of all the potential energy and kinetic energy is an object is equal to its______

due today pls help! :(

Answers

Answer:

total mechanical energy

what is the mass in grams of 0.687 moles of NH three

Answers

NH3 = 14 +3*1=17 g/mol
Mass = mol * molar mass = 0.687 * 17= 11.679 g
Can u mark it brainliest?

A taco from a fast food restaurant contains 7.0 g of fat, 25. g of carbohydrate, and 11 g of protein. How many kJ of energy does the cheeseburger contain? (The caloric values for foods are 38 kJ/g for fat, for carbohydrate, and 17 kJ/g for protein.)

Answers

Answer: 878 kJ of energy is there in cheeseburger

Explanation:

Given : calorific value of fat = 38kJ/g

calorific value of carbohydrate = 17 kJ/g

calorific value of protein = 17kJ/g

1 g of fat contains energy = 38 kJ

7.0 g of fat contains energy = [tex]\frac{38}{1}\times 7.0=266 kJ[/tex]

1 g of carbohydrate contains energy = 17 kJ

25 g of fat contains energy = [tex]\frac{17}{1}\times 25=425kJ[/tex]

1 g of protein contains energy = 17 kJ

11 g of protein contains energy = [tex]\frac{17}{1}\times 11=187kJ[/tex]

Total energy = (266+425+187) kJ = 878 kJ

Give the coefficient of y in the following expression. 2xz² - 7xy + 4.​

Answers

Answer:

the coefficient of y is -7

Why does Hydrogen not belong to any group?

Answers

Answer: Hydrogen is not in any group because it only has on electron

Explanation:

How can weak acids and weak bases cause pH stress to cells?

a. Weak bases will only cause pH stress at low pH.
b. If a cell has transporters that are not well regulated, weak acids or weak bases can accumulate inside the cells and cause stress.
c. Only weak acids can cause stress by diffusing across a membrane at low pH.
d. At certain pH levels, both weak acids or weak bases will be uncharged, and thus are small uncharged molecules that can diffuse across a membrane and cause pH stress inside the cell. e. Weak acids and weak bases do not cause stress.

Answers

Answer:

b

Explanation:

If a cell has transporters that are not well regulated, weak acids or weak bases can accumulate inside the cells and cause stress.

In this stage of team building, the team is running smoothly and they are comfortable in their roles.


norming

performing

forming

storming

Answers

What are you asking?

Answer:

performing

Explanation:

Beryllium oxide, Beo, is an electrical insulator. How
many moles of beryllium oxide qre in a 250 gram
sample of the compound?

Answers

Answer:

There are 10.0 moles of beryllium oxide in a 250 grams sample of the compound.

Explanation:

We can calculate the number of moles (η) of BeO as follows:

[tex] \eta = \frac{m}{M} [/tex]

Where:

m: is the mass = 250 g

M: is the molar mass = 25.0116 g/mol

Hence, the number of moles is:

[tex] \eta = \frac{250 g}{25.0116 g/mol} = 10.0 moles [/tex]

Therefore, there are 10.0 moles of beryllium oxide in a 250 grams sample of the compound.  

I hope it helps you!

How many grams of water are formed if 3.5 moles of ammonia are used?

Answers

Answer : 59.5g

Way to do

Ammonia chemical formula : NH3

Ammonia molar mass : 14 + (1×3) = 17

Mass = Mol × mm

= 3.5mol × 17 = 59.5g

See pic for formula

nvm i think your question is incomplete. pls report my answer i thought u are asking the mass of ammonia

Which process breaks down sugars to release energy that powers bodily functions?

Answers

Answer:

Cellular respiration

Explanation:

A: A 21.3−g sample of dinitrogen monoxide is confined in a 5.76−L vessel. What is the pressure (in atm) at 111°C?

B: Find the density of Freon−11 (CFCl3) at 157°C and 4.65 atm.
g/L = ?

Answers

Answer:

A. 2.65 atm.

B. 18.11 g/L.

Explanation:

A. Determination of the pressure

Mass of N₂O = 21.3 g

Volume = 5.76 L

Temperature (T) = 111 °C

Pressure (P) =.?

First, we shall determine the number of mole in 21.3 g of dinitrogen monoxide, N₂O. This can be obtained as follow:

Mass of N₂O = 21.3 g

Molar mass of N₂O = (14×2) + 16

= 28 + 16

= 44 g/mol

Mole of N₂O =?

Mole = mass /Molar mass

Mole of N₂O = 21.3/44

Mole of N₂O = 0.484 mole

Next, we shall convert 111°C to Kelvin temperature. This can be obtained as follow:

T(K) = T(°C) + 273

Temperature (T) = 111 °C

Temperature (T) = 111 °C + 273

Temperature (T) = 384 K

Finally, we shall determine the pressure. This can be obtained as follow:

Number mole of N₂O = 0.484 mole

Volume = 5.76 L

Temperature (T) = 384 K

Gas constant (R) = 0.0821 atm.L/Kmol

Pressure (P) =.?

PV = nRT

P × 5.76 = 0.484 × 0.0821 × 384

Divide both side by 5.76

P = (0.484 × 0.0821 × 384) / 5.76

P = 2.65 atm

B. Determination of the density of CFCl₃

Temperature (T) = 157°C

Pressure (P) = 4.65 atm.

Density of CFCl₃ =?

First, we shall determine the molar mass of CFCl₃. This can be obtained as follow:

Molar mass of CFCl₃ = 12 + 19 + (35.5×3)

= 12 + 19 + 106.5

= 137.5 g/mol

Next, we shall convert 157°C to Kelvin temperature. This can be obtained as follow:

T(K) = T(°C) + 273

Temperature (T) = 157 °C

Temperature (T) = 157 °C + 273

Temperature (T) = 430 K

Finally, we shall determine the density of CFCl₃. This can be obtained as follow:

Temperature (T) = 430 K

Pressure (P) = 4.65 atm.

Molar mass of CFCl₃ (M) = 137.5 g/mol

Gas constant (R) = 0.0821 atm.L/Kmol

Density (D) of CFCl₃ =?

D = PM / RT

D = (4.65 × 137.5) / (0.0821 × 430)

D = 18.11 g/L

Other Questions
Evaluate the expression. 2.2(2)(14)52.2(2)( 41 )5 Show set of data that is a function using at least 5 domain values and 5 range values. It can be shown in a format of your choice Choose which statement best describes an element.A. Anything that takes up spaceB. A pure substance that cannot be broken down into other substances by chemical means. C. WaterD. Atom has a nucleus with neutrons and protons in it. Which of the following diagrams BEST represents the relationship between galaxies, the Universe, and solar systems? There is a sale on Blu-rays in a local shop 20% off selected items. Your favorite Blu-ray before the sale cost $18. How much will you save? How much will you pay? The students at a high school collected $3,800 to buy stuffed animals to give to a childrens hospital. The students bought both stuffed bears and stuffed dogs. Each bear cost $7, and each dog cost $8. The students bought a total of 500 stuffed animals and spent all the money. How many stuffed dogs did the students buy? A. 200 B. 205 C. 295 D. 300 Choose all items that are true about the two example of HTML shown on the right.Example 1 will display differently than example 2 in a web browser.They are styled differently, but will look the same in a web browser.Example 2 is easier to analyze and repair.The styling in example 2 is required by modern web browsers. F(x) = 3 + 4x G(x) = 6x + 7I) find fg(x) If a strand of DNA has the nitrogen base sequence, GCTAGATGCG, what will bethe sequence of the complementary strand? Does mass alone determine whether an object will float or sink? Explain Please help its urgent How does an organism obtain CO2, H2O, and energy to undergo photosynthesis? create two stanza poem that will inspire the community to recognize the importance of categories of tropical cyclones. Give your poem a title who ruled China in the 19th century? the center of a circle is at (6,7), and the diameter of the circle is 22, which of thr following is the equation of thr circle? ge If 91 is 1% of a number, what is that number? * Simplify the expression. 4x - 2(x - 6) - X el area de un rectangulo es 84 cm cuadrados si la base mide 9 cm cuanto mide la altura y cual es su perimetro? What did Peter call Clarissa that made her wince?A. The angelic motherB. The most articulate housewifeC. The perfect hostessD. A legacy waiting for her future 40. Which two are equivalent to 4?A A 2BV8C V16D V12E V64